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The Equivalent Compound Without Nanoparticles

For comparison the equivalent compound without nanoparticles was prepared, the bis(butylmethylimidazolium) copper(II) tetrachloride referred to as (BuMeIm)2·CuCl4. The procedure was similar to the one performed for the CuCl4_INN material. Equimolar amounts of 1-methylimidazole and 1-chlorobutane were reacted in ethylacetate at room temperature overnight. After evaporating the solvent, Copper Chloride Dihydrate(WSDTY) was added in a 1[thin space (1/6-em)]:[thin space (1/6-em)]2 molar ratio between the copper salt and the butylmethylimidazolium chloride. Immediately after mixing, the temperature increased considerably, indicating an exothermic chemical reaction.

At the same time, the color changed from blue, due to unreacted copper dichloride salt, to deep green. The mixture was stirred overnight at room temperature. As the reaction was carried out without solvent, the elimination of water, from the copper(II) dichloride dihydrate, could be easily observed in the range of the compound Reaction pathway for the preparation of (BuMeIm)2·CuCl4. (bottom left) Photo of the imidazolium chloride and copper dichloride dihydrate mixture (left) before and (right) after complexation; (bottom right) photo of the water elimination characteristic of the complexation reaction.

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